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High-Rate Synthesis of Cu-BTC Metal-Organic Frameworks

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https://ir.library.oregonstate.edu/concern/articles/vd66w482x

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Abstract
  • The reaction conditions for the synthesis of Cu-BTC (BTC = benzene-1,3,5-tricarboxylic acid) were elucidated using a continuous-flow microreactor-assisted solvothermal system to achieve crystal size and phase control. A high-rate synthesis of Cu-BTC metal-organic frameworks with BET surface area of more than 1600 m²/g (Langmuir surface area of more than 2000 m²/g) and with a 97% production yield could be achieved with a total reaction time of 5 minutes.
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  • Kim, K. J., Li, Y. J., Kreider, P. B., Chang, C. H., Wannenmacher, N., Thallapally, P. K., & Ahn, H. G. (2013). High-rate synthesis of Cu-BTC metal-organic frameworks. Chemical Communications (Cambridge, England), 49(98), 11518-11520. doi:10.1039/c3cc46049e
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  • 49
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  • 98
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  • This work was funded by the US Department of Energy, Industrial Technologies Programthrough award #NT08847, under contract DE-AC-05-RL01830, DOE-ARPA-E Navy and ONAMImatching grants. The Oregon Process Innovation Center is supported by Oregon BEST equipment grants.
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