Index Catalog // ScholarsArchive@OSU

Himeradine A : synthetic efforts towards himeradine A and related natural products, a Michael reaction focused approach

Creator:: Collett, Nathan D.
Abstract:: Lycopodium alkaloids have generated enormous amounts of interest from the scientific community, both as synthetic targets and for their medicinal properties. Herein is described work towards a unifying approach to large segments of the Lycopodium family. An organocatalyzed intramolecular heteroatom Michael reaction method, for the construction of piperidine and piperizine...
Resource Type:: Dissertation
Full Text:: 1.8.3 with i-Pr2NH triggered an intramolecular enamine Michael reaction to form cyclohexanone 1.8.4

Development of organocatalyzed, intramolecular heteroatom Michael addition and application towards alkaloid synthesis

Creator:: Carlson, Erik
Abstract:: Effective methods for the enantiopure formation of substituted piperidine rings are significantly important due to their presence in alkaloid products. A valuable method to form these ring systems would be via an intramolecular heteroatom Michael addition from the corresponding enone or enal. Described herein is a methodolgy that has been...
Resource Type:: Masters Thesis
Full Text:: , Intramolecular Heteroatom Michael Addition and Application Towards Alkaloid Synthesis Chapter I

Electrochemical studies of liquid chlorocuprates(I)

Creator:: Silkey, James R.
Abstract:: This research emphasized fundamental physical and electrochemical studies of systems based on the room temperature fused salt, triethyl-ammonium dichlorocuprate(I). Such systems, which must be maintained under a protective atmosphere, were also used in some preliminary battery studies. Spectra of dark green solutions of copper (II) chloride in triethylammonium dichlorocuprate(I) obey...
Resource Type:: Masters Thesis
Full Text:: Electrochemical studies of liquid chlorocuprates(I) AN

Part I.: Reactions of 2-isopropoxymethylene-cyclohexanone with organometallic reagents. Part II.: Thermal rearrangements of ethyl 3-(2-vinylcyclohexen-1-y1) propenoate and 1-vinyl-2-propenylidenecyclohexyl methyl ether

Creator:: Cleary, Michael Franklin
Resource Type:: Dissertation
Full Text:: AN-ALSTRACT OF TLJ:.; Uh313 02 Michael Franklin Clear1 for

New Graphite Intercalation Chemistry with Alkaline Earth Metals

Creator:: Xu, Wei
Abstract:: Novel graphite intercalation compounds (GICs) and associated chemistry have been explored, specifically: (1) containing alkyl- substituted imidazolium cations; (2) a series containing alkaline earth metal (Mg, Ca, Sr, Ba) cations with ethylenediamine (en) co-intercalates; (3) showing reversible intragallery M-M bonding and (4) via electrochemical intercalation of Mg cations with potential...
Resource Type:: Dissertation
Full Text:: Graphite Intercalation Chemistry with Alkaline Earth Metals. Abstract approved: Michael M

Graphite intercalation compounds containing tetra-n-alkylammonium cations

Creator:: Sirisaksoontorn, Weekit
Abstract:: Novel donor-type graphite intercalation compounds (GICs) containing tetra-n-alkylammonium (TAA) cations have been synthesized by using both ion-exchange and electrochemical methods. Structural and compositional data of the resulting TAA-GICs are investigated by using powder X-ray diffraction (PXRD), one-dimensional electron density calculations, thermogravimetric and elemental analyses, and capillary zone electrophoresis (CZE). A...
Resource Type:: Dissertation
Full Text:: Tetra-n-alkylammonium Cations. Abstract approved: Michael M. Lerner Novel donor-type

Gas-phase electron-diffraction investigations of, I. WF₆, ReF₆, OsF₆, IrF₆, PtF₆, O₂⁺PtF⁻₆, II. 3-aminoacrolein, III. 3-chloro-1-propanol, IV. 2,2',5,5'-tetramethyl-1,1'-distibacerrocene

Creator:: Richardson, Alan D.
Resource Type:: Dissertation
Full Text:: Gas-phase electron-diffraction investigations of, I. WF

Intercalation, exfoliation, and nanocomposites of layered inorganic compounds

Creator:: Sukpirom, Nipaka
Abstract:: The melt intercalation of poly(ethylene oxide) (PEO) between layers of MoO₃ and MPS3 (M=Mn,Cd) is obtained by heating the ground mixture and LiₓMoO₃, KₓMn₁-ₓ/₂PS₃, or KCd₁-ₓ/₂PS₃. The products are characterized by powder X-ray diffraction (XRD). Below the melting temperature of PEO (66 °C), intercalation rates and yields are low. By...
Resource Type:: Dissertation
Full Text:: Nanocomposites of Layered Inorganic Compounds. Abstract approved: Michael M. Lerner The melt intercalation of

The synthesis and characterization of novel materials for use in secondary lithium-ion batteries

Creator:: Nafshun, Richard L.
Resource Type:: Dissertation
Full Text:: Characterization of Novel Materials for Use in Secondary Lithium-Ion Batteries. Abstract approved: Michael M

Synthesis, characterization, and structural modeling of graphite intercalation compounds with fluoroanions

Creator:: Yan, Wei
Abstract:: New synthetic strategies have been investigated for nano-dimensioned graphite particles or even isolated graphene sheets. One approach is to prepare graphite intercalation compounds (GICs) with low layer charge density and appropriate gallery height, followed by the colloidal dispersion or exfoliation of the resulting GICs. A series of anions has been...
Resource Type:: Dissertation
Full Text:: : Michael M. Lerner New synthetic strategies have been investigated for nano-dimensioned graphite

ScholarsArchive@OSU

Himeradine A : synthetic efforts towards himeradine A and related natural products, a Michael reaction focused approach

Development of organocatalyzed, intramolecular heteroatom Michael addition and application towards alkaloid synthesis

Electrochemical studies of liquid chlorocuprates(I)

Part I.: Reactions of 2-isopropoxymethylene-cyclohexanone with organometallic reagents. Part II.: Thermal rearrangements of ethyl 3-(2-vinylcyclohexen-1-y1) propenoate and 1-vinyl-2-propenylidenecyclohexyl methyl ether

New Graphite Intercalation Chemistry with Alkaline Earth Metals

Graphite intercalation compounds containing tetra-n-alkylammonium cations

Gas-phase electron-diffraction investigations of, I. WF₆, ReF₆, OsF₆, IrF₆, PtF₆, O₂⁺PtF⁻₆, II. 3-aminoacrolein, III. 3-chloro-1-propanol, IV. 2,2',5,5'-tetramethyl-1,1'-distibacerrocene

Intercalation, exfoliation, and nanocomposites of layered inorganic compounds

The synthesis and characterization of novel materials for use in secondary lithium-ion batteries

Synthesis, characterization, and structural modeling of graphite intercalation compounds with fluoroanions

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