Digital image correlation (DIC) uses pairs of images, one in a reference state and one after in situ manipulation of the object, to measure full-field displacements and strains by tracking the motion of small image subsets. Subset selection is always a crucial part of DIC technique as it has a...
Carbon nanotubes (CNTs) superior mechanical, electrical and thermal properties make them attractive components in nanomechanical devices. Their large aspect ratio and low density makes them ideal candidates for high frequency resonators in numerous applications including wireless communication, and mass and chemical sensors. One reason why CNTs have been slow to...
Microreactors offer high rates of heat transfer able to intensify highly endothermic biomass reforming reactions in supercritical water. In this study, two continuous flow microreactor configurations were used to gasify biomass constituents in supercritical water. The first reactor configuration was a micro diameter stainless steel or Hastelloy tube (508 µm...
Sodium-ion batteries (SIBs) require the use of a highly reversible anode. To form this anode carbon nanofibers and nanocrystals are derived from cellulose nanofibers, cellulose nanocrystals, and bacterial nanocellulose. The primary structure of the cellulose nanofibers is maintained when carbonized allowing for high surface area in the structure. The carbon...
The research presented herein represents an effort to combine the ultra-smooth surface of an amorphous metal thin film (AMTF) with a solution-processed dielectric synthesized via prompt inorganic condensation (PIC). Analysis of dielectric film quality is carried out via electrical measurements of metal-insulator-metal (MIM) diodes. Anneals at 500 and 700 °C...
Metal-organic polyhedra (MOPs) are discrete molecules comprised of a metal and interconnecting ligands. The resulting MOP structures are porous cages, and to date, they have shown great promise toward gas capture. Ammonia is a hazardous gas that is produced in enormous quantities for use in fertilizers. In this talk, I...
In Dual-ion Batteries, anions as charge carriers might be a potential technique of energy storage. While fluoride anion has been selected as a promising charge carrier for energy storage due to its high charge/mass ratio and small ionic radius, carbonate anion has never been reported as a charge carrier for...
Thermal wave imaging (TWI), a technology based on heat conduction and radiation through materials, is a relatively new addition to current non-destructive inspections (NDI) systems. Bonding of composites, an extremely important step in manufacturing and repair of laminates, could be affected by defects originating from faulty manufacturing processes or damages...
As microelectronic parts trend smaller so do their solder joints. The surface finish on a copper pad is expected to become a significant part of the total solder joint volume and therefore affect mechanical properties of the smaller solder joints. Two sample geometries and four different surface finishes for tin-silver-copper...
A Cu/Fe-spinel-based oxygen carrier designed at the National Energy Technology Laboratory was studied in order to characterize its physical and chemical behavior with cyclic oxidation and reduction treatments at 800°C for applications in chemical looping combustions. Observations were made on individual particles of the oxygen carrier in-situ using a confocal...