In this work, continuous synthesis routes for binary nanoparticles using advantages of microchannel mixing (low diffusion distances and higher mass transfer) and fast heating rates provided by ultrasound induced heating are investigated. In addition, the application of silica nanoparticles in anti-reflective coatings on glass and understanding the structure property-performance correlation...
Ceria nanoparticles are of interest owing to their interesting properties like photo-absorption and ability to absorb oxygen. Several batch synthesis routes exist however these methods often lack particle size control, result in agglomeration and typically require high temperature processing. In this paper, a continuous flow microchannel synthesis method based on...
A continuous flow sonochemical reactor was developed capable of producing metastable cadmium sulfide (CdS) nanoplatelets with thicknesses at or below 10 nm. The continuous flow sonochemical reactor included the passive in-line micromixing of reagents prior to sonochemical reaction. Synthesis results were compared with those from reactors involving batch conventional heating...
Advances of colloidal nanomaterials for societal benefit have been hampered by the high cost and low quality of nanoparticles (NPs). The production of high quality nanoparticles within colloidal suspension has two related concerns; (1) current high production rates methods of synthesizing nanoparticles result in a larger range of particle size,...
In the second chapter, a foam-core meniscus coating process was developed for retrofitting 100 nm-scale sol-gel anti-reflective coatings onto in-field solar panels through the deposition, evaporation, and curing of wet films.Advantages of this technique include the means to control fluid flow relative to substrate motion and the ability to conform...
The need for clean and renewable fuel such as hydrogen is driven by a growing worldwide population and increasing air pollution from fossil fuels. One of the major barriers for the use of hydrogen in automotive industry is the storage of hydrogen. Physisorption is the most promising storage technique due...
Microchannel process technology (MPT) offers several advantages to the field of nanomanufacturing: 1) improved process control over very short time intervals owing to shorter diffusional distances; and 2) reduced reactor size due to high surface area to volume ratios and enhanced heat and mass transfer. The objective of this thesis...