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ChangChih-Hung(Alex)ChemicalBiologicalEnvironmentalEngineeringHighRateSynthesis.pdf Public Deposited

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https://ir.library.oregonstate.edu/concern/articles/1j92gc710

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  • The reaction conditions for the synthesis of Cu-BTC (BTC = benzene-1,3,5-tricarboxylic acid) were elucidated using a continuous-flow microreactor-assisted solvothermal system to achieve crystal size and phase control. A high-rate synthesis of Cu-BTC metal-organic frameworks with BET surface area of more than 1600 m²/g (Langmuir surface area of more than 2000 m²/g) and with a 97% production yield could be achieved with a total reaction time of 5 minutes.
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