Graduate Thesis Or Dissertation
 

Synthesis and study of oxides and chalcogenides : thin films and crystals

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  • Several types of solid-state inorganic materials are prepared and characterized. By using the SILAR (Successive Ionic Layer Adsorption and Reaction) deposition method in conjunction with hydrothermal dehydration both low-temperature deposition and crystallization of oxide thin films are achieved. Various aspects of new transparent p-type materials are studied by examining both powders and thin films. Delafossite type compounds, CuMO₂₊₈ (M=Ga, Sc, In), are synthesized by unique methods, yielding single-phase materials. The conductivity, mobility, and carrier concentration in BaCu₂S₂ thin films are described and p-type conductivity in the wide band-gap sulfide fluoride, BaCuSF, is examined. Structural and conducting properties of the various polymorphs of In₂Se₃ and the related structure of Sb₂Te₂Se are considered. Structural characterization and cation ordering in Langasite derivatives, La₃SnGa₅O₁₄ and La₃SnGa₃Al₂O₁₄, is described. Finally, selected aspects of the synthesis, structural characterization, and luminescence properties of Y₃(SiO₄)₂Cl, Mn:Zn₂SiO₄, and Eu:Y₆WO₁₂ are summarized.
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