Graduate Thesis Or Dissertation

 

Synthesis of some bicyclo[6.1.0] - nonane derivatives Public Deposited

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  • Bicyclo [6.1.0] non-4-ene was prepared by two routes; (1) reaction of cis-cis-1, 5-cycloöctadiene with methylene iodide and zinc-copper couple, (2) sodium-methanol reduction of 9, 9-dibromobicyclo-[6.1.0] non-4-ene. The bicyclononene was characterized by its infrared spectrum, nuclear magnetic resonance spectrum and common physical properties. The olefin was hydrogenated to bicyclo [6.1.0] - nonane. 9, 9- Dibromobicyclo [6.1.0] non-4-ene was prepared by dibromocarbene addition to 1, 5-cycloöctadiene. Structure proof was provided by the analytical results, infrared spectrum, nuclear magnetic resonance spectrum and the conversion to bicyclo [6.1.0] non-4-ene. The acetolysis of bicyclo [6.1.0] non-4-ene was carried out and the products analyzed by vapor phase chromatography. At least eight major products were indicated.
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Déclaration de droits
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  • File scanned at 300 ppi using Capture Perfect 3.0 on a Canon DR-9050C in PDF format. CVista PdfCompressor 5.0 was used for pdf compression and textual OCR.
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