Graduate Thesis Or Dissertation
 

High-temperature, high-pressure NMR probe for superconducting magnets

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  • A high-temperature, high-pressure autoclave has been adapted for use with a high-field nuclear magnetic resonance spectrometer. The autoclave has an internal pressure range of atmospheric pressure to 1.5 kbar and a temperature range of 273 K to 1900 K. The autoclave is usable in a high field (8 T) magnet with a room temperature, 76.4 mm bore. The autoclave was tested using assorted nuclear species with resonant frequencies ranging from 57 to 70 MHz at pressures ranging from atmospheric pressure to 1220 bar and temperatures ranging from 273 K to 448 K. Previously, the autoclave was used in conjunction with an iron magnet at temperatures to 1900 K and pressures to 1.5 kbar.
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