Graduate Thesis Or Dissertation

 

Condensation reactions of certain aldehydes and amines with acetylbenzoyl Public Deposited

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  • Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in primary isoamyl alcohol under reflux conditions to form 1,4-diphenvl-3-butene-1,2-dione, compound I, which melted at 56-57°C. Compound I formed a quinoxaline derivative, compound II, which melted at 152.5-153°C. Compound I was cleaved by hydrogen peroxide to form cinnamic acid, compound III, which melted at 133°C. Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in glacial acetic acid under reflux conditions to form 1,4,5-tripheny-1,2,5-pentanetrione, compound IV, which melted at 192-193°C, Compound IV formed an oxime derivative, compound V, which melted at 232-233°C.
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