Condensation reactions of certain aldehydes and amines with acetylbenzoyl

Graduate Thesis Or Dissertation

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Citeable URL: https://ir.library.oregonstate.edu/concern/graduate_thesis_or_dissertations/fq977x156

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Attribute Name	Values
Creator	Klemm, Waldemar Arthur, Jr.
Abstract	Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in primary isoamyl alcohol under reflux conditions to form 1,4-diphenvl-3-butene-1,2-dione, compound I, which melted at 56-57°C. Compound I formed a quinoxaline derivative, compound II, which melted at 152.5-153°C. Compound I was cleaved by hydrogen peroxide to form cinnamic acid, compound III, which melted at 133°C. Acetylbenzoyl reacted with dimethylamine hydrochloride and benzaldehyde in glacial acetic acid under reflux conditions to form 1,4,5-tripheny-1,2,5-pentanetrione, compound IV, which melted at 192-193°C, Compound IV formed an oxime derivative, compound V, which melted at 232-233°C.
Resource Type	Masters Thesis
Date Available	2014-04-18T17:54:59+00:00
Date Issued	1967-05-05
Degree Level	Master's
Degree Name	Master of Science (M.S.)
Degree Field	Chemistry
Degree Grantor	Oregon State University
Commencement Year	1967
Advisor	Logan, A. V.
Academic Affiliation	Chemistry
Non-Academic Affiliation	Oregon State University. Graduate School
Subject	Condensation products (Chemistry)
Declaração de direitos	Copyright Not Evaluated
Publisher	Oregon State University
Peer Reviewed	No
Language	English [eng]
Digitization Specifications	File scanned at 300 ppi using Capture Perfect 3.0 on a Canon DR-9050C in PDF format. CVista PdfCompressor 5.0 was used for pdf compression and textual OCR.
Replaces	http://hdl.handle.net/1957/47467

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