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A study of factors leading to N, N-diacetylation of aminopyrimidines

Creator:: Carson, Bonnie L.
Abstract:: Although 4- and 5-diacetamidopyrimidines have been reported in the literature within the past eleven years, it was not until 1965 that a 2-diacetamidopyrimidine was reported. The current investigation was undertaken to determine whether other 2-diacetamidopyrimi-dines could be synthesized and what the effect of various nuclear substituents would be on the...
Resource Type:: Masters Thesis
Full Text:: presented May 14, 1966 Typed by Gail Dailey ACKNOWLEDGMENT The author is greatly indebted to Dr. B

Preparation and reactions of 7-bicyclo [3.3.1] nonen-2-one

Creator:: Salisbury, Kirby Grant
Abstract:: 2-Carboxy-3(3-cyclohexen-1-yl)propionic acid, 3-(3-cyclohexen-1-yl)propionic acid and 3-(3-cyclohexen-1-yl)propionyl chloride were prepared in sequence from ethyl-2-carbethoxy-3-(3-cyclohexen-1-yl)propionate. Cyclization of 3-(3-cyclohexen-1-yl)propionic acid in polyphosphoric acid resulted in the formation of 4, 5, 6, 7-tetrahydroindanone which was identified by its ultraviolet spectrum and its physical properties. 7-Bicyclo[3.3.1] nonen-2-one was prepared by a Friedel-Crafts cyclization of 3-(3-cyclohexen-1-yl)-propionyl...
Resource Type:: Masters Thesis
Full Text:: identified by its ultraviolet spectrum and its physical properties. 7- Bicyclo[ 3. 3. 1] nonen -2 -one

The study of the influence of the nitro substituent on the hydrazinolysis of certain substituted 5-nitropyrimidines

Creator:: Stahl, Quade Russell
Abstract:: The unique reaction between 4, 6-dimethoxy-5-nitropyrimidine and methylhydrazine was investigated. The reaction product was identified as 4-hydrazino-6-hydroxypyrimidine from (a) spectral data, (b) by direct synthesis of the product via 4-chloro-6-hydroxypyrimidine and hydrazine, and (c) by conversion of the product to the known 4-amino-6-hydroxypyrimidine using Raney nickel. The product was not...
Resource Type:: Dissertation
Full Text:: -hydroxypyrimidine from (a) spectral data, (b) by direct synthesis of the product via 4-chloro-6-hydroxy

Decarboxylation studies on α-methyl-α-Phenylcaproic acid and some of its derivatives

Creator:: Sheppard, Dorothy Louise
Resource Type:: Masters Thesis
Full Text:: 19 same physical constants as the original acid. No decar boxylation resulted. b. One and one

Catalysis of the isotopic exchange reaction between thionyl chloride and liquid sulfur dioxide

Creator:: Burge, David Edwin
Resource Type:: Dissertation
Full Text:: . XPLFiMFfIL ....... 5 A. General Procedure . . . . . 5 B. Radioactivity tneIyais . . . . (d. Chemic1

Addition of hydrogen bromide to unsymmetrical olefins

Creator:: Rogers, Charles Junior
Abstract:: In this investigation the addition of hydrogen bromide to 3-methylcyclohexene has been studied in order to see if the theory of hyperconjugation could be extended to include olefins of this type. Since the olefin has an equal number of hydrogens on both carbons carrying the double bond, a mixture of...
Resource Type:: Dissertation
Full Text:: -brociopentane; this mixture could. not be separated by chemical or physical means since the boiling point of

Methanolysis of tetrakis(trichlorophosphine)nickel(0)

Creator:: Bachman, David Franklin
Abstract:: The methanolysis of phosphorus trichloride coordinated to nickel (0) has been studied. Free phosphorus trichloride reacts with methanol to give dimethyl hydrogen phosphonate, methyl chloride, and hydrogen chloride. The reaction involves a rearrangement on phosphorus using the lone pair, in which the coordination number increases from three to four. In...
Resource Type:: Masters Thesis
Full Text:: extended. Special thanks go to Messrs. G. Gathercoal, O. Barnes, and C. Brown; Mrs. B. Clausen and Mrs

Mechanisms of internal substitution reactions

Creator:: Engebrecht, Ronald Henry
Resource Type:: Dissertation

The Robinson-Mannich base synthesis applied to substituted acetoacetic ester

Creator:: LaPore, Richard Francis
Resource Type:: Dissertation
Full Text:: 6 "> CHa HISTORICAL The reaction between a B - keto ester and a quaternary ammonium salt of

The reaction of N-bromosuccinimide (I) with acetals

Creator:: Joncich, Micheal Joseph
Resource Type:: Masters Thesis
Full Text:: (0.0t5 mole)(7.9 ml.) of product was obtained having the follovdng physical constants: b. p. 40°C. (.01

ScholarsArchive@OSU

A study of factors leading to N, N-diacetylation of aminopyrimidines

Preparation and reactions of 7-bicyclo [3.3.1] nonen-2-one

The study of the influence of the nitro substituent on the hydrazinolysis of certain substituted 5-nitropyrimidines

Decarboxylation studies on α-methyl-α-Phenylcaproic acid and some of its derivatives

Catalysis of the isotopic exchange reaction between thionyl chloride and liquid sulfur dioxide

Addition of hydrogen bromide to unsymmetrical olefins

Methanolysis of tetrakis(trichlorophosphine)nickel(0)

Mechanisms of internal substitution reactions

The Robinson-Mannich base synthesis applied to substituted acetoacetic ester

The reaction of N-bromosuccinimide (I) with acetals

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