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The Electrochemical Synthesis of the Graphite Intercalation Compounds Containing Tetra-n-alkylammonium Cations

Creator:

Sirisaksoontorn, Weekit and Lerner, Michael M.

Abstract:

The electrochemical intercalation of tetra-n-alkylammonium (TAA) cations into graphite is investigated using galvanostatic reduction and cyclic voltammetry in TAABr/ dimethylsulfoxide (DMSO) electrolytes. Structural and compositional analyzes by X-ray diffraction, thermogravimetric and elemental analyzes show that stable graphite intercalation compounds (GICs) are formed with highly-flattened TAA cation bilayers for (C₅H₁₁)₄N⁺, (C₆H₁₃)₄N⁺,...

Resource Type:

Article

Full Text:

) M28-M32 (2013) 2162-8769/2013/2(9)/M28/5/$31.00 © The Electrochemical Society The Electrochemical