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Filtering by: Creator McMichael, John Seiple Remove constraint Creator: McMichael, John Seiple Academic Affiliation Chemistry Remove constraint Academic Affiliation: Chemistry

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Total Synthesis of Goniomitine : Development of Aminal and α-Amino Radicals in the Synthesis of Nitrogen-Rich Natural Products

Creator:

Vellucci, Jessica K.

Abstract:

Aminal radical intermediates were generated by the method of radical translocation and reacted in C-C bond forming reactions with electronically deficient alkenes (Schiedler et al. Org. Lett. 2012, 14, 6092). Aminal radical intermediates can participate in inter- and intra-molecular reactions using both Bu3SnH and (TMS)₃SiH as hydride donors. Carbon–carbon bonds...

Resource Type:

Dissertation

Full Text:

, M.; Grube, A.; Seiple, I. B.; Baran, P. S. Angew. Chem. Int. Ed. 2007, 46, 6586. For a review on
The development of aminal radicals for the synthesis of nitrogen-rich natural products

Creator:

Schiedler, David A.

Abstract:

Organic compounds which contain one or more nitrogen atoms are especially important as they are disproportionately represented among biologically active molecules. As a result, significant effort has been focused on the development of methods for the synthesis of nitrogenous molecules. We identified the aminal as an under-explored functional group. Despite...

Resource Type:

Dissertation
The investigation of octaammine-μ-nitro-μ-amidodicobalt (III) nitrate as an analytical reagent for sulfate

Creator:

Dennison, James Eugene

Resource Type:

Masters Thesis

Full Text:

and 14]. kept at room temperature, about n well and filtered through A seiple of each solution
The aromatic Cope rearrangement : energetics and reality

Creator:

Almond, Stephen W.

Resource Type:

Dissertation
Thermal [pi]-route rearrangement of 4-cycloheptane-1-methyl acetate

Creator:

Schick, Lawrence Edward

Abstract:

Pyrolysis of 4-cycloheptene-l-methyl acetate under flow conditions at 285° gives only rearranged bicyclic acetates and hydrocarbons rather than the anticipated simple elimination product methylenecyclohept- 4-ene. These rearranged acetates have the same structures and are formed in virtually the same relative percentages as those observed in the "π- route" solvolysis of...

Resource Type:

Dissertation

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Academic Affiliation

Chemistry[remove]5

Advisor

Beaudry, Christopher M.2
Marvell, Elliot N.1
Thies, Richard W.1
Williams, Max B.1

Commencement Year

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Current results range from 1962 to 2015

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Committee Member

Blakemore, Paul R.2
Baham, John E.1
Burrows, Sean M.1
Cheong, Paul H. Y.1
Cheong, Paul H.-Y.1
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Creator

Almond, Stephen W.1
Dennison, James Eugene1
Schick, Lawrence Edward1
Schiedler, David A.1
Vellucci, Jessica K.1

Date

Date range begin – Date range end

Current results range from 1962 to 2015

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Decade

2010-20192
1970-19792
1960-19691

Degree Field

Chemistry5

Degree Level

Doctoral4
Master's1

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Doctor of Philosophy (Ph.D.)4
Master of Science (M.S.)1

Language

English [eng]5

License

All rights reserved2

Non-Academic Affiliation

Oregon State University. Graduate School5

Peer Reviewed

No5

Resource Type

Dissertation4
Masters Thesis1

Rights Statement

Copyright Not Evaluated3
In Copyright2

Subject

Amino groups2
Alkaloids -- Synthesis1
Aromatic compounds1
Chemical tests and reagents1
Natural products1
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