The effect of cosputtered catalyst on growth and alignment of carbon nanotubes (CNTs) grown by plasma enhanced chemical vapor deposition (PECVD) was investigated. Aligned CNTs were observed using a cosputtered catalytic metal deposited directly on boro-aluminosilicate glass. Catalytic metal alloys were sputtered directly onto the substrate using magnetron sputtering. Deposition...
Cobalt germanides have been widely studied as semiconductor contact materials, but recent theoretical studies suggest that they may also be excellent catalysts for methane steam reforming with stabilities and activities comparable to noble metal catalysts. In order to study the catalytic activity of cobalt germanides, it is critical to first...
Cubic phase Li₇La₃Zr₂O₁₂ (LLZO) is a promising solid electrolyte for all solid-state lithium-ion battery, due to its reasonable ionic conductivity, stable against metallic Li, wide chemical window, and thermal and chemical stability. The main aim of this thesis is to investigate the influences of different synthesis methods on the structure...
In Intense Pulsed Light (IPL) sintering, pulsed large-area visible light from a xenon lamp is absorbed by nanoparticle films or patterns and converted to heat, resulting in rapid sintering of the nanoparticles. This work experimentally characterizes IPL sintering of silver nanoparticle films. A newly observed turning point in the evolution...
Influences of operating conditions on the production of carbon nanotubes
(CNTs) were studied using Fe and Fe-Ni bimetallic catalysts supported on silicon
monoxide (SiO). The catalysts were prepared in three steps: (1) impregnation of SiO
powders with ferric nitride or combinations of ferric and nickel nitrides, (2) oxidation
of nitrides...
PDMS membrane-based microvalves are becoming increasingly more important for the control of fluid flow within MECS applications such as microreactors used to synthesize nanoparticles and biological macromolecules. The motivation for pursuing PDMS membrane-based microvalves is for implementing a plug flow microreactor to simulate slug flow yielding a narrower residence time...