The reaction conditions for the synthesis of Cu-BTC (BTC = benzene-1,3,5-tricarboxylic acid) were elucidated using a continuous-flow microreactor-assisted solvothermal system to achieve crystal size and phase control. A high-rate synthesis of Cu-BTC metal-organic frameworks with BET surface area of more than 1600 m²/g (Langmuir surface area of more than 2000...
Solution deposition offers an attractive, low temperature option in the cost effective production of thin film solar cells. Continuous microreactor-assisted solution deposition (MASD) was used to produce nanocrystalline cadmium sulfide (CdS) films on fluorine doped tin oxide (FTO) coated glass substrates with excellent uniformity. We report a novel liquid coating...
The role of gold nanoparticles supported on ZnO in photocatalytic activity for dye degradation
was investigated. To do this, gold nanoparticles supported on ZnO (Au-ZnO) were prepared using a
simple co-precipitation method. The prepared nanocatalyst was characterized by high resolution
transmission electron microscopy, X-ray diffraction, temperature programmed reduction, X-ray
photoelectron...
Continuous microreactor-assisted solution deposition is demonstrated for the deposition
of CdS thin films on fluorine-doped tin oxide (FTO) coated glass. The continuous flow
system consists of a microscale T-junction micromixer with the co-axial water circulation
heat exchanger to control the reacting chemical flux and optimize the heterogeneous surface
reaction. Dense,...
Copper sulfides (CuxS) are compound semiconductor materials that exhibit considerable variations of optical and electrical properties. Copper sulfide thin films can be used in many applications, such as solar control coatings, solar cells, photothermal conversion of solar energy, electroconductive coatings, and microwave shielding coatings. In this paper, chemical bath deposition...
Assembly of nanocrystals is considered one of the most promising approaches to design nano-, microstructures, and complex mesoscopic architectures. A variety of strategies to induce nanocrystal assembly have been reported, including directed assembly methods that apply external forces to fabricate assembled structures. In this study ZnO nanocrystals were synthesized in...
Cerium oxide nanoparticles were continuously
precipitated from a solution of cerium(III) nitrate and ammonium
hydroxide using a static microchannel T-mixer. Tmixer
synthesis results were compared with synthesis results
from batch precipitation. Findings show that the method of
mixing is important in the ceria precipitation process. Uniform
porous film structures and...