The temporal and spatial characteristics of the plume produced
by a laser microprobe, are dependent upon the composition and pressure
of the atmosphere surrounding it. It has been shown that certain atmospheres
can enhance the analytical signal by increasing the free
atom lifetime.
Improvements were made to the existing laser...
¹³⁰ Sn and ¹²⁸Sn were separated from mixed fission products.
The decay of these isotopes were studied with Ge(Li),
LEPS, and plastic scintillator detector systems in single
and two parameter coincidence modes. The decay scheme constructed
for ¹²⁸Sn decay has levels at 0.0 (5+), 45.7 (4+),
77.8 (3+), 152.9 (2+),...
Solubility studies on the heavy metal sulfides in liquid hydrogen
sulfide at room temperature were carried out using the isopiestic
method. The results were compared with earlier work and with a
theoretical result based on Raoult's Law. A relative order for the
solubilities of sulfur and the sulfides of tin,...
Thermal analysis was used to investigate the following seven
systems: H₂S-B₂F₄, SOF₂-B₂F₄, COC1₂-B₂F₄, SF₄-B₂F₄, Xe-BF₃, NF₃-BF₃, and NF₃-BC1₃. In two of the seven systems
compound formation was observed.
In the system, H₂S-B₂F₄ the compounds H₂S[superscript .]B₂F₄ and
2H₂S[superscript .]B₂F₄ are formed. The compound H₂S[superscript .]B₂F₄ has a melting
point of...
Attempts to synthesize diboron tetrafluoride by the reduction of
boron trifluoride with alkali metal solutions in 1, 2-dimethoxyethane
proved to be unsuccessful. No diboron tetrahalide was found when
boron trifluoride, antimony trifluoride, or boron trichloride was
reacted with tetra-(dimethylamino)-diboron; although there appeared
to be some exchange between chloride and amine...