Index Catalog // ScholarsArchive@OSU

Creator:: Luo, Wei, Wang, Xingfeng, Meyers, Colin, Wannenmacher, Nick, Sirisaksoontorn, Weekit, Lerner, Michael M., and Ji, Xiulei
Abstract:: Magnesiothermic reduction can directly convert SiO₂ into Si nanostructures. Despite intense efforts, efficient fabrication of highly nanoporous silicon by Mg still remains a significant challenge due to the exothermic reaction nature. By employing table salt (NaCl) as a heat scavenger for the magnesiothermic reduction, we demonstrate an effective route to...
Resource Type:: Article
Full Text:: Enabled by a Heat Scavenger in Magnesiothermic Reactions Wei Luo1, Xingfeng Wang1, Colin Meyers2, Nick

Creator:: Albuquerque, Gustavo H., Fitzmorris, Robert C., Ahmadi, Majid, Wannenmacher, Nick, Thallapally, Praveen K., McGrail, B. Peter, and Herman, Gregory S.
Abstract:: The metal organic framework, MOF-74(Ni), was synthesized in a continuous flow microwave-assisted reactor obtaining a high space-time yield (~90 g h⁻¹ L⁻¹) and 96.5% conversion of reagents. Separation of the nucleation and growth steps was performed by using uniform and rapid microwave heating to induce nucleation, which allowed a substantial...
Resource Type:: Article
Full Text:: Gustavo H. Albuquerque,a Robert C. Fitzmorris,a Majid Ahmadi,a Nick Wannenmacher,a Praveen K. Thallapally

Creator:: Kim, Ki-Joong, Li, Yong Jun, Kreider, Peter B., Chang, Chih-Hung, Wannenmacher, Nick, Thallapally, Praveen K., and Ahn, Ho-Geun
Abstract:: The reaction conditions for the synthesis of Cu-BTC (BTC = benzene-1,3,5-tricarboxylic acid) were elucidated using a continuous-flow microreactor-assisted solvothermal system to achieve crystal size and phase control. A high-rate synthesis of Cu-BTC metal-organic frameworks with BET surface area of more than 1600 m²/g (Langmuir surface area of more than 2000...
Resource Type:: Article

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