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Creator:: Whitman, James Edgar
Abstract:: The purpose of this project was to study the reactions of 1-(α-pyridyl)-3-buten-1-ol (compound I) and to determine whether or not the products of some of its reactions are quinolizinium salts. Reaction of compound I with bromine or iodine yields halide salts (when no external cooling is applied) instead of the...
Resource Type:: Masters Thesis
Full Text:: 2860 I 585 I 560 1460 t430 I400 r330-r300 r145 TT?3 I 100 33 Cornpo,nnd Bands (.rrr- 1) I -( c

Creator:: Ladwig, Laurence Gene
Abstract:: The reaction of certain purin-8-ols with phosphorus oxychloride and N,N-diethylaniline are described. 9-Amino-6-chloropurin-8-ol monohydrate reacted with phosphorus oxychloride and N, N-diethylaniline to yield the phosphorus oxychloride adduct. Other purin-8-ols were prepared and the production of analogs similar to the previously mentioned adduct was attempted. 6-Chloropurin-8-ol and 6, 9-diaminopurin-8-ol hydrochloride monohydrate...
Resource Type:: Masters Thesis
Full Text:: . (Nujol has absorption peaks at approximately 2920, 2860, 1460, and 1375 cm, l). The ultraviolet

Creator:: Kaesornsomboon, Somkid
Resource Type:: Masters Thesis
Full Text:: . -1 (phenyl), 1450 cm. -1, 1460 cm. -1(S02 asymmetric stretch), and 1175 cm. -1(SOz symmetric stretch

Creator:: Rogers, Charles Junior
Abstract:: In this investigation the addition of hydrogen bromide to 3-methylcyclohexene has been studied in order to see if the theory of hyperconjugation could be extended to include olefins of this type. Since the olefin has an equal number of hydrogens on both carbons carrying the double bond, a mixture of...
Resource Type:: Dissertation
Full Text:: Loyse (24, pp.1460-i) prepared the olefin by the action o alcoholic potash bu 3-bromopentane and

Creator:: Rusay, Ronald Joseph
Abstract:: The retro-ene reaction of 2-vinylcyclohexanols occurs readily in the vapor phase at 400-450° producing unsaturated carbonyl compounds in good yields. The starting- materials were prepared in general by the carbenoid addition reaction of ethyl diazoacetate, appropriately substituted cyclohexene, and copper catalyst to produce bicyclic esters which were reduced to the...
Resource Type:: Dissertation

Creator:: Carson, Bonnie L.
Abstract:: Although 4- and 5-diacetamidopyrimidines have been reported in the literature within the past eleven years, it was not until 1965 that a 2-diacetamidopyrimidine was reported. The current investigation was undertaken to determine whether other 2-diacetamidopyrimi-dines could be synthesized and what the effect of various nuclear substituents would be on the...
Resource Type:: Masters Thesis

Creator:: Stahl, Quade Russell
Abstract:: The unique reaction between 4, 6-dimethoxy-5-nitropyrimidine and methylhydrazine was investigated. The reaction product was identified as 4-hydrazino-6-hydroxypyrimidine from (a) spectral data, (b) by direct synthesis of the product via 4-chloro-6-hydroxypyrimidine and hydrazine, and (c) by conversion of the product to the known 4-amino-6-hydroxypyrimidine using Raney nickel. The product was not...
Resource Type:: Dissertation

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