This report is one of a series issued in cooperation with the ANC-23 Panel on Composite Construction for Flight Vehicles of the Departments of the Air Force, Navy, and Commerce.
We present a new method developed for measuring radiocarbon of methane (¹⁴CH₄) in ancient air samples
extracted from glacial ice and dating 11,000–15,000 calendar years before present. The small size (~20 μg CH₄ carbon), low
CH₄ concentrations ([CH₄], 400–800 parts per billion [ppb]), high carbon monoxide concentrations ([CO]), and low...